M.Pharm-M.Pharm Pharmaceutical Analysis 3rd Year Pharmaceutical Analysis(Kerala University of Health Sciences-2014)

QP CODE:302326                                                   Reg.No: ……………………..
Third Year Pharm D Degree Supplementary Examinations - April 2014
Pharmaceutical Analysis

Time: 3 Hours                                                                                                           Total Marks: 70

• Answer all Questions.

• Draw Diagrams wherever necessary.

Essays (3x10=30)

1. Enumerate the qualities that are desirable for a gas that is used as GC mobile
phase. Explain the principle and applications of affinity chromatography.
2. Explain the construction and working of any one HPLC detector With a neat
diagram. Discuss the various methods of preparation of TLC plate.
3. Explain Beer-Lambert’s law and mention its limitations. Explain the different
chromatographic development technique employed in paper chromatographic
technique.
Short notes (8x5=40)
4. Explain the construction and working of differential scanning calorimeter
5. Explain the principle and applications of atomic absorption spectroscopic
technique.
6. Explain the sample preparation technique for solid samples in IR spectroscopic
analysis.
7. Explain the reciprocal lattice technique.
8. ICH guidelines
9. Explain the methods of detection of end point in potentiometry
10. Explain the principle and application of amperometric technique
11. Explain the principle of electrophoresis technique and mention its applications.
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