M.Pharm-M.Pharm Pharmaceutical Analysis 3rd Year Pharmaceutical Analysis(Kerala University of Health Sciences-2013)

QP CODE:302326                              Reg.No: ……………………..
Third Year Pharm D Degree Examinations - October 2013
Pharmaceutical Analysis

Time: 3 Hours                                                                                                          Total Marks: 70

• Answer all Questions.

• Draw Diagrams wherever necessary.

Essays (3x10=30)

1. Discuss the factors affecting resolution in a chromatographic technique. Explain
construction and working of injection port of an HPLC.
2. Compare and contrast TLC technique with HPTLC technique. Mention the
detectors used in GC and explain the working of any one detector
3. Discuss the effect of solvent and pH on UV absorption spectra. Discuss the factors
affecting fluorescence.
Short notes (8x5=40)
4. Explain the construction and working of a pH meter.
5. Compare amperometry with potentiometry
6. Explain the factors affecting polarographic wave.
7. Explain the advantages and disadvantages of electron impact ionization technique
8. Explain the steps involved in equipment validation
9. Explain the principle and applications of atomic absorption spectrometry.
10. Discuss the applications of DSC technique.
11. Explain the electronic transitions taking place when a molecule is exposed
to ultraviolet visible radiation
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