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Biju Patnaik University of Technology 2008-6th Sem B.Pharm BPham Pharmaceutical Analysis-II - Question Paper

Thursday, 23 May 2013 06:20Web



Total number of printed pages - 4 B. Pharm

PH. 6.7

Sixth Semester Examination - 2008 PHARMACEUTICAL ANALYSIS - II Full Marks-70


Time: 3 Hours

aps'j

1. united stand,..


Answer Question No. 1 which is compulsory and any five from the rest.

The figures in the right-hand margin indicate marks.

1. Answer all questions :

2x10


(a)    What is the basic difference between iodimetry and iodometry ?

(b)    How can you determine the qualitative and quantitative analysis by polarography ?

(c)    Define Residual Current.

(d)    Write the various errors in coulometric titrations.

(e)    Calculate the equivalent weight of potassium permanganate in acidic medium.

(f)    Give an example of oxidation-reduction reaction in which sodium 2,6 - dichloro-phenol indophenol is used.

(g)    Name the various electrodes that are used for determining the pH.

(h)    What is oxygen flask combustion gaso-metry ?

(i)    Write the advantages and disadvantages of conductometric titrations.

(j) Which kind of reaction occurs in Karl-

Fischer titrations ?


(a)    Theory of redox titrations

(b)    Electrophoresis.

3. Define polarography. Write down the instrumentation and important applications of polaro

graphy.    10

4.    What are the advantages and disadvantages of amperometric titrations ?    10

5.    Write short notes on :    5+5

(a)    Radioimmuno assays

(b)    Kjeldahl method of nitrogen estimation.

6. Write the instrumentation and applications of a

pH meter.    10

7.    Write short notes on :    5+5

(a)    Diazotisation titrations

(b)    Oxidation-reduction indicators.

8.    Write the principles, instrumentation and applications of Potentiometric titrations. 10

PH. 6.7    4    -C







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